PEG purification of PCR products
Modified from a protocol by Travis Glenn at Univ. South Carolina
Do not use for PCR products less than 300bp.
- Set heatblock/water bath to 37C.
- Run 2 uL of PCR product on a minigel to ensure the reaction worked.
- Add 50 uL (for 50uL PCR reactions) of PEG to a 0.7 mL tube. Add the remainder of the PCR product and mix by pipetting up & down.
- Incubate at 37C for 15 minutes.
- Centrifuge (max speed) 15 minutes.
- Pipette off the liquid and discard it. Careful–the pellet probably won’t be visible.
- Add 125 uL ice cold 80% EtOH
- Centrifuge 2 minutes.
- Pipette off the liquid and discard it.
- Repeat steps 7-9.
- Dry 15-30 minutes in a speedvac if available–otherwise air-dry, spinning briefly every few minutes to ensure the final droplet doesn’t “climb” the tube as it evaporates). There should be no trace of liquid or EtOH odor.
- Spin briefly to ensure DNA is at the bottom of the tube.
- Add 25uL TE buffer (10mM Tris, 0.1mM EDTA recipe). Mix by pipetting.
- Incubate at 37C for 5 minutes.
- Turn off heatblock/waterbath
- Quantify on Nanodrop.
Recipes
PEG for purification of PCR products
20% PEG, 2.5 M NaCl
- For 50mL (enough for ~1000 PCR reactions) mix the following in a 100mL Pyrex bottle:
- 10.0 g PolyEthylene Glycol 8000 (MW = 6000 - 8000 is fine)
- 7.3 g NaCl
- ddH2O up to ~45 mL
- Stir with magnetic rod on lowest heat. PEG may not completely dissolve depending on how much water you’ve added, but after 20-30 minutes, fill with ddH2O up to 50 mL and mix until completely dissolved.
- Store in the refrigerator.
Note- This recipe is good for PCR products larger than 300bp. Increasing PEG or NaCl concentrations will allow smaller products.